Carbonaceous contaminants on support films for transmission electron microscopy
نویسنده
چکیده
Evaporated carbon support films for transmission electron microscopy often contain carbonaceous contaminants. These include poorly graphitized carbon, fragments of graphite, and fullerene-like structures such as nanotubes and nanoparticles. In some cases, carbyne crystals may also be present. There are many examples in the carbon literature where these contaminants have been mistaken for sample material. This paper describes the kinds of contaminants observed on grids obtained from a number of commercial suppliers. 2001 Elsevier Science Ltd. All rights reserved.
منابع مشابه
Carbon nanotubes and other graphitic structures as contaminants on evaporated carbon films
High-resolution electron microscopy (HREM) has been widely used in studies of fullerene-related carbons, and in particular has been applied extensively to the study of carbon nanotubes (Iijima, 1991; Ebbesen & Ajayan, 1992) and carbon nanoparticles (Harris et al., 1993; Saito et al., 1993). The purpose of this Note is to draw the attention of workers in this field to the fact that carbon nanotu...
متن کاملInfluence of CVD process duration on morphology, structure and sensing properties of carbonaceous- palladium films
We present the nanocomposite carbonaceous-palladium (C-Pd) thin films prepared by physical vapor deposition (PVD) and chemical vapor deposition (CVD) methods. Scanning electron microscope (SEM) and transmission electron microscope (TEM) methods were used to study the topography, morphology and structure of carbon and palladium nanograins contained in these films. The quantitative analysis of th...
متن کاملThe production of carbon nanofibers and thin films on palladium catalysts from ethylene–oxygen mixtures
The characteristics of carbonaceous materials deposited in fuel rich ethylene–oxygen mixtures on three types of palladium: foil, sputtered film, and nanopowder, are reported. It was found that the form of palladium has a dramatic influence on the morphology of the deposited carbon. In particular, on sputtered film and powder, tight ‘weaves’ of sub-micron filaments formed quickly. In contrast, o...
متن کاملThe micro-distribution of carbonaceous matter in the Murchison meteorite as investigated by Raman imaging.
The carbonaceous Murchison chondrite is one of the most studied meteorites. It is considered to be an astrobiology standard for detection of extraterrestrial organic matter. Considerable work has been done to resolve the elemental composition of this meteorite. Raman spectroscopy is a very suitable technique for non-destructive rapid in situ analyses to establish the spatial distribution of car...
متن کاملMorphological Characterization of Combustion Deposited Diamond Crystals and Films
Single crystals and polycrystalline diamond films of several thicknesses were deposited using oxygen/acetylene combustion flame technique. The substrate used was pure polycrystalline molybdenum subjected to mechanical polishing. Quality and microstructural characteristic of diamond produced were investigated using X-Ray diffraction, Raman Spectroscopy, Scanning and Transmission Electron Microsc...
متن کاملذخیره در منابع من
با ذخیره ی این منبع در منابع من، دسترسی به آن را برای استفاده های بعدی آسان تر کنید
عنوان ژورنال:
دوره شماره
صفحات -
تاریخ انتشار 2000